9-Fluorenylmethoxycarbonylpyroglutamate, a side-product of derivatization of glutamate with 9-fluorenylmethyl chloroformate: a warning.

Details

Request a copyRequest a copy
Serval ID
serval:BIB_197387882A7A
Type
Article: article from journal or magazin.
Collection
Publications
Institution
Production externe
Title
9-Fluorenylmethoxycarbonylpyroglutamate, a side-product of derivatization of glutamate with 9-fluorenylmethyl chloroformate: a warning.
Journal
Analytical biochemistry
Author(s)
Keller H.J., Quang Do K., Zollinger M., Winterhalter K.H., Cuénod M.
ISSN
0003-2697 (Print)
ISSN-L
0003-2697
Publication state
Published
Issued date
01/11/1987
Peer-reviewed
Oui
Volume
166
Number
2
Pages
431-434
Language
english
Notes
Publication types: Journal Article ; Research Support, Non-U.S. Gov't
Publication Status: ppublish
Abstract
9-Fluorenylmethyl chloroformate derivatization is widely used for determinations of amino acids in biological material. The derivatization of glutamate leads to the formation of 9-fluorenylmethoxycarbonylpyroglutamate as a side-product, which is thus a methodological artifact.

Keywords
Amino Acids/analysis, Animals, Brain Chemistry, Chromatography, High Pressure Liquid, Fluorenes/analysis, Glutamates/analysis, Mass Spectrometry, Pyrrolidinones/analysis, Pyrrolidonecarboxylic Acid/analogs & derivatives, Pyrrolidonecarboxylic Acid/analysis, Rats
Pubmed
3434783
Web of science
A1987K752100026
Create date
06/03/2014 17:18
Last modification date
20/08/2019 13:50
Usage data